基于碳纳米管/Ag/MoS2转导层的全固态钙离子选择电极

构建了一种电势稳定性好的全固态钙离子选择电极(Ca²⁺-ISE),采用碳纳米管(CNT)/Ag/MoS₂为转导层,自制的三脚架化合物作为钙离子载体,制备固体接触式Ca²⁺-ISE。 系统分析了全固态Ca²⁺-ISE的稳定性、能斯特斜率、响应范围、选择性系数等主要性能,发现制备的固体接触式Ca²⁺-ISE在钙离子浓度为1×10^-6~1×10^-1 mol/L范围内呈现线性能斯特响应,响应斜率为28.1 mV/decade。 CNT/Ag/MoS₂的引入有利于提高固体接触式Ca²⁺-ISE的离子浓度线性响应范围,缩短电势平衡时间,降低测试能斯特斜率与理论值差,对于Ca²⁺-ISE的长期在线检测有重要研究意义。     

Determining the optimal pre-tightening force of a sandwich transducer by measuring resonance resistance

The pre-tightening force applied on a sandwich transducer plays a key role on the transducer’s vibration performance. Typically, a transducer’s optimal pre-tightening force is not known during assembly. The objective of this study is to examine a method for determining the optimal pre-tightening force for a sandwich transducer. We propose that the transducer’s optimal pre-tightening force can be measured indirectly through the resonance resistance. Resonance resistance is an equivalent electric parameter which reflects the transducer’s mechanical energy loss, and can be measured easily using an impedance analyzer. The relationship between resonance resistance and the pre-tightening force is analyzed both theoretically and experimentally. Measurement of resonance resistance based on transducer’s admittance circle is studied. Experiments involving this relationship are conducted. Results indicate that the front-end surface amplitude of the sandwich transducer reaches a maximum when the pre-tightening force is optimal, the resonance resistance tends to a minimum, but with a small offset. This indicates that the minimum value of resonance resistance corresponds closely to the highest vibration amplitude of the transducer, but not exactly. Thus, by determining the minimum resonance resistance, the optimal pre-tightening force can be determined.     

硅油介质中矩形电容式微机械超声换能器发射与接收声场特性研究

与传统压电式超声换能器相比,基于微机电系统微加工技术制备的电容式微机械超声换能器(CMUT)具有频带宽、灵敏度高、一致性好、易于集成等优势,在医学超声成像中具有广阔的应用前景。该文针对研制的矩形CMUT器件,开展硅油介质中CMUT发射、接收声场特性的理论分析及实验验证研究。首先,针对CMUT阵元结构特征和工作原理,根据指向性函数理论和Bridge乘积原理,建立了矩形CMUT阵元指向性函数分析模型。此基础上,分析微元数目以及谐振频率对CMUT指向性的影响规律。最后,针对7 mm×7 mm二维矩形CMUT在硅油介质中的发射和接收特性进行了实验验证,测试表明发射指向性曲线与仿真理论曲线基本吻合;此外,CMUT接收与发射指向性的测试表明,收发指向性具有一致性,从而验证了声场的互易性。该文的研究对CMUT器件的封装设计以及基于CMUT阵列的乳腺超声CT成像系统的研制具有重要参考价值。     

面向CMUT声发射特性的驱动电路优化设计

根据电容式微机械超声换能器(CMUT)的工作原理,设计了用于驱动CMUT发射超声波的电路.通过适当的串行匹配,消除了脉冲激励信号的过冲现象.在此基础上进一步探究了脉冲激励参数对CMUT声发射特性影响.结果表明,随着激励脉冲个数的增加,CMUT输出超声信号的有效带宽逐渐变窄,二次谐波逐渐增强;随着激励脉冲占空比的增加,C...     

Nonlinearity analysis of piezoelectric micromachined ultrasonic transducers based on couple stress theory

This paper studies the static deformation behavior of a piezoelectric micromachined ultrasonic transducer (PMUT) actuated by a strong external electric field. The transducer membrane consists of a piezoelectric layer, a passive layer and two electrode layers. The nonlinearities of the piezoelectric layer caused by electrostriction under a strong electric field are analyzed. Because the thickness of the transducer membrane is on the microscale, the size dependence of the deformation behavior is evaluated using the couple stress theory. The results show that the optimal ratio of the top electrode diameter and the membrane diameter is around 0.674. It is also found that this optimal value does not depend on any other parameters if the thicknesses of the two electrodes are negligible compared with those of the piezoelectric and passive layers. In addition, the nonlinearities of the piezoelectric layer will become stronger along with the increase of the electric field, which means that softening of the membrane stiffness occurs when a strong external electric field is applied. Meanwhile, the optimal thickness ratio for the passive layer and the piezoelectric layer is not equal to 1.0 which is usually adopted by previous researchers. Because there exists size dependence of membrane deformation, the optimal value of this thickness ratio needs to be greater than 1.0 on the microscale.     

宽光谱AOTF匹配网络对光谱衍射效率影响的研究

基于声光可调滤波器(acousto-optic tunable filter,AOTF)光谱成像分析仪在可见至红外光谱的多个谱区内广泛应用,对AOTF的光谱带宽及衍射效率提出了更高的要求。超声换能器作为AOTF的核心部件,其3 dB工作带宽决定AOTF的光谱衍射范围,故在同一声光介质上制作两片厚度不同的换能器来提高AOTF光谱带宽。由于超声换能器在不同频率下具有不同的输入阻抗,当驱动信号源输出阻抗与超声换能器输入阻抗失配时会产生能量损耗,导致无法把功率最大限度的传递给超声换能器,从而使AOTF光谱衍射效率降低,影响光谱成像清晰度。通过射频电路先进设计系统(ADS)仿真及实验测试,设计了一种新型宽带阻抗匹配网络,在60～200 MHz带宽范围内,阻抗匹配网络功率效率达到90％以上,光谱衍射效率最高达90％,提高了在420～1 150 nm波段内的光谱灵敏度。     

氢气/丙烷/空气预混气体爆轰性能的实验研究

通过采用压力传感器和烟灰板两种测试设备,开展了常温常压下氢气/丙烷和空气混合气体爆轰性能的实验研究。实验过程中观察到自持爆轰波,爆轰速度比值在0.99~1之间,爆轰压力比值在0.8~1.2之间。爆轰胞格尺寸在10~50 mm范围内,建立了爆轰胞格尺寸和化学诱导长度的关系式。随着丙烷不断添加,爆轰速度减小,而爆轰压力和胞格尺寸增加。这种变化趋势起初较快,而后变缓。因为起初氢气摩尔分数较大,混合气体趋向于氢气/空气的爆轰性能;而后因丙烷摩尔质量较大,丙烷逐渐起主要作用,混合气体表现出丙烷/空气的爆轰性能。     

压电陶瓷非线性对大功率换能器结构参数匹配影响的计算分析

在Guyomar非线性模型基础上,通过机电等效法将晶堆前向负载作为等效质量和阻尼加入振动方程的质量项和阻尼项,推导了换能器振速、辐射声压级和谐振频率偏移率等表达式,计算分析了压电陶瓷非线性参数和结构参数对换能器声辐射性能的影响,研究了压电陶瓷的非线性对换能器结构参数匹配的影响。结果表明,换能器节面靠前,前盖板厚度越小,前盖板大径越小,都可以减少压电陶瓷非线性引起的换能器频率偏移。当设计频率确定时,压电陶瓷处于非线性工作域的换能器的结构参数有所减小。换能器加入辐射端匹配后,可以改善压电晶堆前向负载匹配,降低换能器的谐振频率偏移率。换能器激励电流也会出现频率偏移现象。在提高换能器激励电压时,换能器的结构参数应适当减小。得到的结论可为换能器设计提供理论依据和帮助。     

超声测距变结构控制系统的研究

本文在超声测距系统中采用了变结构控制理论，根据所测物体的反射界面和介质性质，自动调节超声波发射换能器的功率，建立了超声测距系统的数学模型，对系统方程进行了理论分析，研究了变结构控制系统的设计方法，并结合应用实例，对钻井法凿井用超声波测井仪中超声测距系统进行了计算机仿真，并在实验室进行了实验。